I'm using Chemstation for LC 3d Systems Rev B.04.03 with unique folder creation turned on. After an impurities run, I have gone through and done all necessary manual integration through the navigation pane and saved it with the data file each time. I'd like to see a batch file that included my manual integration but this doesn't seem possible since I didn't do the manual integration within the batch. Alternately, I'd like to be able to output a summary report similar to the batch report without using a batch.
1 Introduction to Agilent ChemStation Rev B.04.02 SP1. This chapter. Al brooks trading price action reversals pdf. New functionality is described in detail in the user manuals and in the online help.
Preferably the summary report would be in Excel format, or in a format that is easy to copy into Excel. All I need in the report is the Compound name, area, retention time and height, laid out horizontally like it would be in a batch report.
Any suggestions? I should note the following: I'm in a research environment, manual integration is definitely acceptable The method is looking for drug impurities and potential leachables from a medical device. The sample injection volume is high so that the imputies peaks show up, the two main compounds in the samples are not of interest. Manual integration is necessary because the chromatograms are often so entirely different among samples that a single set of integration parameters cannot be made to work for all samples.
The reason I'd like to know this: this is my first time using this version of chemstation where manual integration changes done in the navigation pane and stored with the data file are completely seperate from manual integration done when reviewing the batch. I did not know this, I thought that if I did all my manual integration in the navigation pane and saved it to the each data file then when I opened the core batch file it would contain the manual adjustments. This is not the case. Even if I reprocess the data with the manual integration saved to each data file, which re-creates the core.b batch file, the batch will not contain the manual integration. The problem is that I've already done 16 runs over 10 weeks of a 26 week stability study and I don't want to have to go back and open each run as a batch and then re-do the manual integration for all ~6000 samples when I already have the integration done and saved with the data file. But I can't see any way to get anything equivalent to the batch report based on the modified data files. I'm not able to get sequence summary reporting to do it right, even as a text file (sequence summary reports won't print as Excel files).
And I don't even know where to begin with macros. Any help would be greatly appreciated, I'm looking at having to re-do about 3 weeks of work here. If you make changes in main(acquisition) method for manual integration and save it.
After that in Preferences menu go to Signal/Review options and mark in Field 'Method used for review of Sequence data/Single run data' -Current Method. From now on when your method is opened and You open data file, should be integrated as You specified in original method ( main method for analyses on samples). That is my way of working.
I hope so to help. Thank you Danail Y. For providing this response through LinkedIN.
1.0 OBJECTIVE: To lay down the procedure for operation and calibration of High Performance Liquid Chromatograph. 2.0 INSTRUMENT IDENTIFICATION: Name of Instrument: High Performance Liquid Chromatography (Auto Sampler) Manufacturer: AGILENT Technologies 1260 series 3.0 GENERAL CLEANING: 3.1 Ensure that the power supply to the instrument is switched off and main Cord is removed from supply. 3.2 Clean the instrument with a clean dry cloth every day.
A wet cloth dipped In dilute soap solution may be used occasionally. 3.3 Precaution must be taken to clean the instrument immediately with dry Cloth after wet cleaning. 4.0 PROCEDURE (OPERATION) 4.1 Ensure that the HPLC system is placed in a clean and dust free area. 4.2 Ensure that instrument have been connected to the main power unit. 4.3 Switch ‘ON’ the Computer.
4.4 Switch ‘ON’ the HPLC instrument. (Switch on the detector, column compartment, Pump and vacuum degasser simultaneously).
4.5 Ensure that the outlet from the detector dips into a waste bottle. 5.0 Start the Open Lab Chemistration by double-clicking the Short cute Open Lab Chemistration located on your desktop. 5.1 Click on Open Lab Chemistration online.
5.2 Then click on ‘on’ option. 5.3 Initialization process of HPLC system will be start which shows by yellow colour.
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